| 254 | 1 | 42 |
| 下载次数 | 被引频次 | 阅读次数 |
采用多道次搅拌摩擦加工技术(MFSP)对冷喷涂增材制造(CSAM)6061铝合金进行大面积加工改性。采用SEM、EBSD和XRD对CSAM试样和MFSP试样不同区域的微观组织进行了表征,并利用显微硬度和室温拉伸测试对其力学性能进行了研究。结果表明,CSAM试样存在大量微孔、裂纹缺陷,晶粒分布不均匀,大角度晶界占比仅为41.4%。相比CSAM试样,MFSP试样晶粒均匀并细化至2.09μm,大角度晶界占比升高至78.0%,位错密度显著降低。其中,加工区和界面区的晶粒分别细化至2.31和1.86μm,大角度晶界占比分别升高至72.8%和83.1%。相比加工区,界面区晶粒细化程度和大角度晶界占比更高,这是由于界面区经历了重复机械搅拌和热作用,促进了连续动态再结晶。MFSP试样平均显微硬度、极限抗拉强度和伸长率分别为58 HV、177 MPa和14.5%,相比CSAM试样分别提高了35%、101%和753%。
Abstract:The cold spray additive manufactured(CSAM) 6061 aluminum alloy was modified in a large area by multi-pass friction stir processing(MFSP). The microstructures of different zones of the CSAM sample and the MFSP sample were characterized by SEM, EBSD and XRD, and their mechanical properties were investigated by microhardness and tensile at room temperature tests. The results show that a large number of micropores and cracks are displayed in the CSAM samples, with an uneven grain distribution and a high proportion of high-angle grain boundaries(41.4%). Compared with the CSAM sample, the grains of the MFSP sample are more uniform and refined to 2.09 μm, the proportion of high-angle grain boundaries is increased to 78.0%, and the dislocation density is significantly reduced. The grains in the processed zone and interfacial zone are refined to 2.31 and 1.86 μm, and the proportions of high-angle grain boundaries are increased to 72.8% and 83.1%, respectively. The grain refinement and the proportion of high-angle grain boundaries in the interfacial zone are higher than those in the processed zone, which is attributed to the repeated mechanical stirring and thermal effects in the interfacial zone, promoting continuous dynamic recrystallization. The microhardness, ultimate tensile strength and elongation of the MFSP sample are 58 HV, 177 MPa and 14.5%, respectively, which represent improvements of 35%, 101% and 753% compared with the CSAM sample.
[1] RANA J K,SIVAPRAHASAM D,RAJU K S,et al.Microstructure and mechanical properties of nanocrystalline high strength Al-Mg-Si (AA6061) alloy by high energy ball milling and spark plasma sintering[J].Materials Science and Engineering:A,2009,527(1-2):292-296.
[2] TANG E L,WANG D,LI L,et al.Polarization response characteristics of 6061Al and PMMA sheets under impact load[J].International Journal of Impact Engineering,2023,178:104632.
[3] ROMETSCH P A,ZHU Y M,WU X H,et al.Review of high-strength aluminium alloys for additive manufacturing by laser powder bed fusion[J].Materials & Design,2022,219:110779.
[4] YIN S,CAVALIERE P,ALDWELL B,et al.Cold spray additive manufacturing and repair:Fundamentals and applications[J].Additive Manufacturing,2018,21:628-650.
[5] 崔烺,刘光,冯胜强,等.冷喷涂增材制造技术研究现状及应用与挑战[J].稀有金属材料与工程,2023,52(1):351-373.CUI Lang,LIU Guang,FENG Shengqiang,et al.Research status,application and challenges of cold spray additive manufacturing technology[J].Rare Metal Materials and Engineering,2023,52(1):351-373.
[6] XIE X L,CHEN C Y,CHEN Z,et al.Achieving simultaneously improved tensile strength and ductility of a nano-TiB2/AlSi10Mg composite produced by cold spray additive manufacturing[J].Composites Part B:Engineering,2020,202:108404.
[7] LIU F C,FENG A H,PEI X,et al.Friction stir based welding,processing,extrusion and additive manufacturing[J].Progress in Materials Science,2024,146:101330.
[8] JI G,LIU H,YANG G J,et al.Improving adhesion strength and electrical conductivity of cold-sprayed Al deposit on Cu substrate through friction-stir-processing[J].Journal of Thermal Spray Technology,2022,31:1813-1826.
[9] SOVA A,GORIAINOVA I,FEULVARCH E,et al.Comparison between friction stir processing and laser remelting processes of cold sprayed metallic composite coatings[J].Materials Letters,2023,349:134898.
[10] WANG W,HAN P,WANG Y H,et al.High-performance bulk pure Al prepared through cold spray-friction stir processing composite additive manufacturing[J].Journal of Materials Research and Technology,2020,9(4):9073-9079.
[11] LIU Z H,HAN P,WANG W,et al.Microstructure,mechanical properties,and corrosion behavior of 6061Al alloy prepared by cold spray-friction stir processing composite additive manufacturing[J].Transactions of Nonferrous Metals Society of China,2023,33(11):3250-3265.
[12] 叶东明,韩鹏,王文,等.CoCrFeNi/6061Al复合材料冷喷摩擦复合增材制造及增强相影响规律研究[J].塑性工程学报,2024,31(3):206-213.YE Dongming,HAN Peng,WANG Wen,et al.Research on cold spray-friction stir processing composite additive manufacturing of CoCrFeNi/6061Al composites and influence law of reinforcement phase[J].Journal of Plasticity Engineering,2024,31(3):206-213.
[13] 王俣豪,乔柯,张兵,等.冷喷摩擦复合增材制造制备ZrO2颗粒增强钛基复合材料组织与磨损性能[J].塑性工程学报,2024,31(2):105-112.WANG Yuhao,QIAO Ke,ZHANG Bing,et al.Microstructure and tribological properties of ZrO2 particles reinforced titanium matrix composites prepared via cold spray-friction composite additive manufacturing[J].Journal of Plasticity Engineering,2024,31(2):105-112.
[14] GUAN X H,WANG W,ZHANG T,et al.A new insight into LPSO phase transformation and mechanical properties uniformity of large-scale Mg-Gd-Y-Zn-Zr alloy prepared by multi-pass friction stir processing[J].Journal of Magnesium and Alloys,2024,12(5):2041-2056.
[15] YIN S,MEYER M,LI W Y,et al.Gas flow,particle acceleration,and heat transfer in cold spray:A review[J].Journal of Thermal Spray Technology,2016,25(5):874-896.
[16] NASCIMENTO F,SANTOS T,VILACA P,et al.Microstructural modification and ductility enhancement of surfaces modified by FSP in aluminium alloys[J].Materials Science and Engineering A,2009,506(1-2):16-22.
[17] EVANS W C,DAN X D,HOUSHMAND A,et al.Microstructural characterization of aluminum 6061 splats cold spray deposited on aluminum 6061-T6 substrate[J].Metallurgical and Materials Transactions A,2019,50(8):3937-3948.
[18] TARIP N H,GYANSAH L,QIU X,et al.Achieving strength-ductility synergy in cold spray additively manufactured Al/B4C composites through a hybrid post-deposition treatment[J].Journal of Materials Science and Technology,2019,35(6):1053-1063.
[19] RUI S S,HAN Q N,WANG X,et al.Correlations between two EBSD-based metrics kernel average misorientation and image quality on indicating dislocations of near-failure low alloy steels induced by tensile and cyclic deformations[J].Materials Today Communications,2021,27:102445.
[20] TIAN X,CHEN F,JIANG J N,et al.Experimental analyses and numerical modeling of the microstructure evolution of aluminum alloy using an internal state variable plasticity-based approach coupled with the effects of second phase[J].International Journal of Plasticity,2022,158:103416.
[21] CHEN Y,DING H,MALOPHEYEV S,et al.Influence of multi-pass friction stir processing on microstructure and mechanical properties of 7B04-O Al alloy[J].Transactions of Nonferrous Metals Society of China,2017,27(4):789-796.
[22] AL-FADHALAH K J,ALMAZROUEE A I,ALORAIER A S.Microstructure and mechanical properties of multi-pass friction stir processed aluminum alloy 6063[J].Materials & Design,2014,53:550-560.
[23] HUANG R Z,SONE M,MA W H,et al.The effects of heat treatment on the mechanical properties of cold-sprayed coatings[J].Surface and Coatings Technology,2015,261:278-288.
基本信息:
中图分类号:TG146.21;TG453.9
引用信息:
[1]段佳兴,韩鹏,王文,等.多道次搅拌摩擦加工改性冷喷涂增材制造6061铝合金微观组织及力学性能[J].塑性工程学报,2025,32(12):194-201.
基金信息:
国家自然科学优秀青年科学基金资助项目(52222410); 国家自然科学基金面上项目(51974220); 陕西省杰出青年科学基金资助项目(2022JC-24); 中央引导地方科技发展资金资助项目(2024ZY-JCYJ-04-09)
2025-12-29
2025-12-29
2025-12-29