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在空气及水介质中对Mg-Gd-Y-Zn-Zr合金进行搅拌摩擦加工(FSP),分析了加工区的组织形貌特征,并研究了加工过程中不同冷却介质对加工区组织性能的影响。结果表明,空气中和水下FSP试样的平均晶粒尺寸分别为4和2μm。在空气中及水下FSP过程中,试样的大角度晶界比例提高,织构显著弱化。温度曲线表明:空气中FSP试样的持续热输入时间和冷却速率分别为49 s和8.5℃·s-1,水下FSP试样为23 s和30.7℃·s-1。由于水下FSP试样热输入的减少对再结晶过程的影响,其试样组织中的亚结构比例高于空气中FSP试样。同时,水下FSP试样保留了更多均匀分布的LPSO相。空气中FSP试样的屈服强度和抗拉强度分别为213和315 MPa,水下FSP试样分别为334和393 MPa。此外,所有FSP试样无力学性能各向异性。
Abstract:Mg-Gd-Y-Zn-Zr alloy was processed by friction stir processing(FSP) in air and water medium, the microstructure morphologies characteristics of the processing zones were analyzed and the effects of different cooling media on the structure properties of the processing zones were studied. The results show that the average grain sizes of the samples processed in air and underwater are 4 and 2 μm, respectively. In the process of FSP in air and underwater, the proportion of large angle grain boundary increases and the texture is weaken significantly. The temperature curves show that the duration heat input time and cooling rate of the FSP samples in air are 49 s and 8.5 ℃·s-1, respectively, and 23 s and 30.7 ℃·s-1 of FSP samples underwater, respectively. Due to the influence of the reduction of heat input for FSP samples underwater on the recrystallization process, the proportion of substructures of FSP samples underwater is higher than that of FSP samples in air. At the same time, more evenly distributed LPSO phases are retained in FSP samples underwater. The yield strength and tensile strength of FSP samples in air are 213 and 315 MPa, respectively, and 334 and 393 MPa of samples underwater, respectively. In addition, all FSP samples show no anisotropy of mechanical property.
[1] WEI X X,LI J,LIU C L,et al.Effect of pack-forging on microstructure and properties of Mg-Gd-Y-Zn-Zr alloy [J].Materials Science and Engineering:A,2021,802:140674.
[2] XIA X S,ZHANG K,MA M L,et al.Microstructures and strengthening mechanisms of Mg-8.2Gd-4.6Y-1.5Zn-0.4Zr alloy containing LPSO,β′ and γ type phases [J].Journal of Rare Earths,2020,38:1119-1125.
[3] JIN X Z,XU W C,YANG Z Z,et al.Analysis of abnormal texture formation and strengthening mechanism in an extruded Mg-Gd-Y-Zn-Zr alloy [J].Journal of Materials Science & Technology,2020,45:133-145.
[4] 苏鹏,李兵兵,靳丽,等.可溶压裂球和桥塞用GW104+1Zn镁合金挤压组织和性能研究[J].塑性工程学报,2021,28(1):122-130.SU Peng,LI Bingbing,JIN Li,et al.Study on extrusion microstructure and properties of GW104+1Zn magnesium alloy for soluble fracturing ball and bridge plug[J].Journal of Plasticity Engineering,2021,28(1):122-130.
[5] ZHENG L Z,LIU C M,WAN Y C,et al.Microstructures and mechanical properties of Mg-10Gd-6Y-2Zn-0.6Zr(wt.%) alloy [J].Journal of Alloys and Compounds,2011,509:8832-8839.
[6] XIA X S,CHEN Q,LI J P,et al.Characterization of hot deformation behavior of as-extruded Mg-Gd-Y-Zn-Zr alloy [J].Journal of Alloys and Compounds,2014,610:203-211.
[7] 邱宇,孟强,董继红,等.6061-T6铝合金搅拌摩擦焊工艺及性能研究 [J].塑性工程学报,2021,28(2):86-91.QIU Yu,MENG Qiang,DONG Jihong,et al.Study on technology and properties of friction stir welding for 6061-T6 aluminum alloy [J].Journal of Plasticity Engineering,2021,28(2):86-91.
[8] WANG W,HANG P,PENG P,et al.Friction stir processing of magnesium alloys:A review [J].Acta Metallurgica Sinica(English Letters),2020,33:43-57.
[9] JIN Y Y,WANG K S,WANG W,et al.Microstructure and mechanical properties of AE42 rare earth-containing magnesium alloy prepared by friction stir processing [J].Materials Characterization,2019,150:52-61.
[10] LI B,HOU X X,TENG B G.Effects of friction stir process and subsequent aging treatment on the microstructure evolution and mechanical properties of Mg-Gd-Y-Zn-Zr alloy[J].Materials Characterization,2019,155:109832.
[11] YANG Q,XIAO B L,WANG D,et al.Formation of long-period stacking ordered phase only within grains in Mg-Gd-Y-Zn-Zr casting by friction stir processing [J].Journal of Alloys and Compounds,2013,581:585-589.
[12] YANG Q,XIAO B L,WANG D,et al.Study on distribution of long-period stacking ordered phase in Mg-Gd-Y-Zn-Zr alloy using friction stir processing [J].Materials Science and Engineering:A,2015,626:275-285.
[13] WANG K,WANG J F,HUANG S,et al.Enhanced mechanical properties of Mg-Gd-Y-Zn-Mn alloy by tailoring the morphology of long period stacking ordered phase [J].Materials Science and Engineering:A,2018,733:267-275.
[14] XU C,NAKATA T,FAN G H,et al.Microstructure and mechanical properties of extruded Mg-Gd-Y-Zn alloy with Mn or Zr addition [J].Journal of Materials Science,2019,54:10473-10488.
[15] CHEN X Y,DAI Q,LI X C,et al.Microstructure and tensile properties of friction stir processed Mg-Sn-Zn alloy [J].Materials,2018,11(4):645.
[16] DATTA A,WAGHMARE U,RAMAMURTY U.Structure and stacking faults in layered Mg-Zn-Y alloys:A first-principles study [J].Acta Materialia,2008,56:2531-2539.
[17] TANE M,SUZUKI S M,YAMASAKI M,et al.Insignificant elastic-modulus mismatch and stress partitioning in two-phase Mg-Zn-Y alloys comprised of α-Mg and long-period stacking ordered phases [J].Materials Science and Engineering:A,2018,710:227-239.
[18] HE J H,JIN L,WANG F H,et al.Mechanical properties of Mg-8Gd-3Y-0.5Zr alloy with bimodal grain size distributions [J].Journal of Magnesium and Alloys,2017,5:423-429.
[19] LI Y X,YANG C L,ZENG X Q,et al.Microstructure evolution and mechanical properties of magnesium alloys containing long period stacking ordered phase [J].Materials Characterization,2018,141:286-295.
[20] MATSUDA M,ANDO S,NISHIDA M.Dislocation structure in rapidly solidified Mg97Zn1Y2 alloy with long period stacking order phase [J].Materials Transactions,2005,46:361-364.
[21] XU C,NAKATA T,QIAO X G,et al.Ageing behavior of extruded Mg-8.2Gd-3.8Y-1.0Zn-0.4Zr (wt.%) alloy containing LPSO phase and γ′ precipitates [J].Scientific Reports,2017,7:43391.
[22] ZHOU X J,XIONG W Y,ZENG G,et al.Combined effects of LPSO orientation and α-Mg texture on tensile anisotropy of an extruded Mg-Gd-Y-Zn-Zr alloy [J].Materials Science and Engineering:A,2021,805:140596.
基本信息:
中图分类号:TG146.22
引用信息:
[1]关肖虎,王文,张婷,等.水下搅拌摩擦加工对Mg-Gd-Y-Zn-Zr合金微观组织和力学性能的影响[J],2023,30(01):191-199.
基金信息:
陕西省重点研发计划(2020ZDLGY13-06)